Desomorphine synthesis
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A facile and improved synthesis of desomorphine and its deuterium-labeled analogue. Journal: Monatshefte für Chemie
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by JN Winborn 2024Synthesis of desomorphine using α-chlorocodide. In 2024 Perrine and Small published their attempts to improve the synthesis of desomorphine (47). They first
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(7) desomorphine;. 6.11. (8) dihydromorphine origin or independently by means of chemical synthesis, or by a combination of extraction.
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Krokodil was produced mimicking street synthesis followed by addicts. Desomorphine was synthesized using the hydriodic acid/red phosphorous reduction.
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The traditional synthesis of desomorphine starts from α-chlorocodide, which is itself obtained by treating codeine with thionyl chloride.
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(g) Desomorphine;. 78. (h) Dihydromorphine;. 79. (i) Drotebanol;. 80. (j) 265 synthesis, or by combination of extraction and chemical synthesis: 266.
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Alves, The harmful chemistry behind krokodil (desomorphine) synthesis and mechanisms of toxicity, Forensic Sci. Int, № 249C, с. 207
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synthesis, or by a combination of extraction and chemical synthesis: (1) Desomorphine. Dihydromorphine. Etorphine. Heroin. Hydromorphinol.
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Abstract This work describes a convenient and improved process for the synthesis of desomorphine from codeine. The proposed method affords the highly pure opiate without the aid of chromatographic purification, and provides a simple route for the synthesis of [2H3] deuterium-labeled desomorphine. Graphical abstract
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Thanks a bunch!!!!!!!!!!!!
Synthesis
Anyway, gave it 4 stars for the concept, plot and grammar.